Electric Power ›› 2022, Vol. 55 ›› Issue (2): 200-208.DOI: 10.11930/j.issn.1004-9649.202007232

• Application of New Materials in Power Systems • Previous Articles     Next Articles

Heat-Treatment Optimizing Study on Soft Magnetic Properties of FeCuNbSiB Nanocrystalline Alloys

DONG Bangshao1,3, ZHOU Shaoxiong1,2, ZHI Qizheng3, XING Yanxing2, YANG Fuyao4, QIAO Guangyao4, HAN Yu4   

  1. 1. Advanced Technology & Materials Co., Ltd., Beijing 100081, China;
    2. Jiangsu JITRI Advanced Energy & Materials Research Institute Co., Ltd., Changzhou 213032, China;
    3. School of Materials and Metallurgy, Northeastern University, Shenyang 110004, China;
    4. Global Energy Interconnection Research Institute Co., Ltd., Beijing 102209, China
  • Received:2020-08-10 Revised:2020-12-22 Online:2022-02-28 Published:2022-02-23
  • Supported by:
    This work is supported by the National Key R&D Program of China (No.2017YFB0903903) and the National Natural Science Foundation of China (No.51971093).

Abstract: This job was focused on the annealing technique of large-size nanocrystalline core with height of 50 mm, to meet the low core loss requirement of large-size nanocrystalline core used in large-capacity high-frequency transformer. Two typical nanocrystalline alloys, Fe73.5Cu1Nb3Si15.5B7 and Fe73.5Cu1Nb3Si13.5B9 ribbons (hereinafter referred to as B7 and B9) with the width of 50 mm, were selected to investigate the influence of annealing temperatures (330~600℃) on their soft magnetic properties and core losses. The experimental results were demonstrated that B7 and B9 alloys probably started to crystallize as early as annealed at 420 ℃, which is much lower temperature than the widely-held at 500 ℃. The two alloys were obtained the lowest core losses by being annealed at 550℃ and 580℃, respectively. However, they showed the highest permeability and the lowest coercivity when annealed at 500℃ and 550℃, respectively. The core losses of B7 alloy was continued to reduce through by transversal field annealing, and the lowest value of Pcm(0.5T/20k) was 7.3W/kg, which is the lowest as far as we know. According to the measured data, the core losses of nanocrystalline magnetic core can be described by $ {P}_{{\rm{cm}}}=0.5{f}^{1.42}{{B}_{{\rm{m}}}}^{2.27} $ in fractional method, and has been confirmed by experimental results.

Key words: nanocrystalline alloy, core loss, annealing temperature, large-capacity high-frequency transformer, fractional method